(R)-(-)-2-PHENYLGLYCINE CHLORIDE HYDROCHLORIDE

Name	D-(-)-A-phenylglycine acid chloride hydrochloride
Synonyms	D(-)-Phenyl Glycine HCl d-phenylglycinechloridehydrochloride D-alpha-Phenylglycine chloride hydrochloride D-(-)-Phenylglycineacidchloride,hydrochloride (R)-(-)-2-PHENYLGLYCINE CHLORIDE HYDROCHLORIDE (R)-(-)-2-Phenylglycine chloride hydrochloride (-)-alpha-(chloroformyl)benzylammonium chloride D-(-)-A-phenylglycine acid chloride hydrochloride (R)-ALPHA-AMINOPHENYLACETYL CHLORIDE HYDROCHLORIDE (R)-.alpha.-Aminobenzeneacetylchloride,hydrochloride .alpha.-amino-,hydrochloride,(R)-Benzeneacetylchloride Benzeneacetylchloride,.alpha.-amino-,hydrochloride,(R)- alpha-amino-,hydrochloride,(theta)-benzeneacetylchlorid
CAS	39878-87-0
EINECS	254-668-5
InChI	InChI=1/C8H8ClNO.ClH/c9-8(11)7(10)6-4-2-1-3-5-6;/h1-5,7H,10H2;1H/t7-;/m1./s1

Molecular Formula	C8H9Cl2NO
Molar Mass	206.07
Melting Point	117°C (dec.)(lit.)
Boling Point	247.2°C at 760 mmHg
Flash Point	302°F
Solubility	Dimethylsulfoxide, Water
Vapor Presure	0.026mmHg at 25°C
Appearance	Powder
Color	Pale brown
Storage Condition	Inert atmosphere,Room Temperature
Sensitive	Moisture Sensitive
Use	For the synthesis of semi-synthetic penicillins and cephalosporins

Hazard Symbols	C - Corrosive
Risk Codes	R22 - Harmful if swallowed R34 - Causes burns R42 - May cause sensitization by inhalation
Safety Description	S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection. S45 - In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
UN IDs	UN 3261 8/PG 2
WGK Germany	3
RTECS	CY1920000
FLUKA BRAND F CODES	10-19-21-34
TSCA	Yes
Hazard Class	8

EPA chemical information	Information provided by: ofmpub.epa.gov (external link)
uses	intermediates for the synthesis of semi-synthetic penicillin and cephalosporins antibiotics pioneer I, pivoxil ampicillin, ampicillin, etc.
production method	put DL-phenylglycine into the split tank, add water and D-camphor sulfonic acid, and heat. Activated carbon decolorization, filtration, cooling, precipitation crystallization. Crystallization is added with 4 times the amount of water, heated and dissolved, ammonia is neutralized, and cooled to obtain D(-)-phenylglycine. D(-)-phenylglycine and ethyl acetate were added to a chlorination pot, hydrogen chloride was passed on 5-10 for about 3h, phosphorus pentachloride was added, reacted at 15 ℃ for 5h, filtered, and the filter cake was washed with ethyl acetate to obtain phenylyl chloride hydrochloride.

Last Update：2024-04-09 20:52:54

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